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A compact, ultrahigh vacuum, radiative heater based on pyrolytic boron nitride that efficiently directs nearly all of its radiation to the sample was designed and constructed. It is shown that the heater reaches temperatures of 1300 K experimentally at 60% of its maximum power. A COMSOL Multiphysics® simulation and an analytical model predict an ultimate temperature of up to 1500 K. Furthermore, the heater does not introduce any contamination to the sample. This is accomplished by a custom-made Nb radiation shield, which was manufactured by selective laser melting and holds a flag-style sample holder. Before manufacturing, the whole assembly was simulated with COMSOL Multiphysics to validate the design of the radiation shield.We demonstrate that under ambient and humidity-controlled conditions, operation of bimodal excitation single-scan electric force microscopy with no electrical feedback loop increases the spatial resolution of surface electrical property measurements down to the 5 nm limit. This technical improvement is featured on epitaxial graphene layers on SiC, which is used as a model sample. The experimental conditions developed to achieve such resolution are discussed and linked to the stable imaging achieved using the proposed method. The application of the herein reported method is achieved without the need to apply DC bias voltages, which benefits specimens that are highly sensitive to polarization. Besides, it allows the simultaneous parallel acquisition of surface electrical properties (such as contact potential difference) at the same scanning rate as in amplitude modulation atomic force microscopy (AFM) topography measurements. This makes it attractive for applications in high scanning speed AFM experiments in various fields for material screening and metrology of semiconductor systems.In this paper, we report studies of the Fermi potential and loss per bounce of ultracold neutrons (UCNs) on a deuterated scintillator (Eljen-299-02D). These UCN properties of the scintillator enable its use in a wide variety of applications in fundamental neutron research.In this study, the application of micro-leverage in the monolithically all-quartz resonant accelerometer is proposed. The magnification of the micro-leverage structure used for a large size double-ended tuning fork (DETF) was analyzed. The effect of DETF's dimension both on its own force-frequency sensitivity and micro-leverage's magnification was investigated. Through the study of the relationship between DETF's force-frequency sensitivity and micro-leverage's magnification, the effect of micro-leverage and the DETF system on the sensitivity of the accelerometer was obtained. The problem of big error in theoretical calculation of micro-leverage magnification was solved because the structural arrangement of the output beam was ignored in the derivation process. The correctness of the analysis was verified by theoretical calculation, simulation, and the experiment. The equivalent structures of tension (compression) stiffness and flexural stiffness of the micro-leverage output beam were obtained by analyzing and simplifying the composite structure of the link beam and DETF. TL13-112 cell line By simplifying the mechanical model of micro-leverage, the amplification factor K of micro-leverage is deduced to be 23. Therefore, the theoretical sensitivity of the sensor is 15.6 Hz/g. The experimental results show that the sensitivity of the accelerometer with the micro-leverage is 16.1 Hz/g, which is close to the theoretical analysis results.Dispersion interferometry (DI) is a promising method for density measurement. Compared with the traditional interferometer, the DI is immune to mechanical vibration and can avoid the fringe jump error. In addition, a simple optical configuration is also one of the advantages of the DI. The electron density of the Huazhong University of Science and Technology field-reversed configuration (HFRC) device can reach 1020 m-3 with a pulse length of 50 µs. In this case, the DI based on the CO2 laser on the HFRC device adopts the heterodyne technique based on the acousto-optic modulator, which can increase the temporal resolution to 40 MHz. It can realize density fluctuation measurements in the MHz range. The test of each optical element, especially the nonlinear crystal, has been completed. The AgGaSe2 crystal can produce a second harmonic wave of about 52.5 µW when the incident CO2 power is 10 W. Based on these designs and tests, a DI system can be expected on the HFRC device.In this article, we propose a method for improving accuracy in calibrating Leeb hardness testers using fiber interferometric systems. The calibration system is implemented using the photonic Doppler velocimetry technique. This paper provides estimates of the measurement uncertainty arising in the calibration system and describes a method for improving accuracy, which takes into account the signal-to-noise ratio, sampling rate, and processing parameters.A linear cryogenic 16-pole wire ion trap has been developed and constructed for cryogenic ion spectroscopy at temperatures below 4 K. The trap is temperature-variable, can be operated with different buffer gases, and offers large optical access perpendicular to the ion beam direction. The housing geometry enables temperature measurement during radio frequency operation. The effective trapping potential of the wire-based radio frequency trap is described and compared to conventional multipole ion trap designs. Furthermore, time-of-flight mass spectra of multiple helium tagged protonated glycine ions that are extracted from the trap are presented, which prove very low ion temperatures and suitable conditions for sensitive spectroscopy.Differential dynamic microscopy (DDM) is increasingly used in the fields of soft matter physics and biophysics to extract the dynamics of microscopic objects across a range of wavevectors by optical microscopy. Standard DDM is limited to detecting dynamics no faster than the camera frame rate. We report on an extension to DDM where we sequentially illuminate the sample with spectrally distinct light and image with a color camera. By pulsing blue and then red light separated by a lag time much smaller than the camera's exposure time, we are able to use this two-color DDM method to measure dynamics occurring much faster than the camera frame rate.
My Website: https://www.selleckchem.com/products/tl13-112.html
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