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Odeslání zprávy. The best conditions for chiral separation Fmoc-D-Phe-OH and Fmoc-L-Phe-OH Can you give me detailed info, step by step ? at least two or three way
Hledá se: „chiral separation Fmoc-D-Phe-OH and Fmoc-L-Phe-OH“
Hledá se: „chiral separation Fmoc-D-Phe-OH and Fmoc-L-Phe-OH“
Hledá se: „chiral separation methods“
Hledá se: „chiral separation methods“
Generování odpovědí pro vás…
Generování odpovědí pro vás…
Dobrý den, tady je Bing. Rád vám pomohu. 😊
Chiral separation is the process of separating two enantiomers of a molecule that have different optical activities. There are many methods for chiral separation, such as liquid chromatography1, capillary electrophoresis2, and supercritical fluid chromatography3. These methods use different chiral selectors or reagents that interact selectively with the enantiomers to form complexes or derivatives with different mobilities or retention times.
For Fmoc-D-Phe-OH and Fmoc-L-Phe-OH, I found one study that used a novel D-camphoric acid-based MOF (metal-organic framework) as a chiral selector for liquid chromatography4. The study reported that the MOF 1 could separate racemic phenylalanine with a resolution of 2.01 and an enantioselectivity of 1.24 after 24 hours at 25 °C.
Another study investigated the self-assembly of Fmoc-D-Phe-L-Phe-OFm and Fmoc-L-Phe-L-Phe-OFm in different solvents56. The study found that heterochirality restricted the structural diversity and polymorphism of the dipeptides compared to homochirality. The study suggested that this could be exploited for chiral recognition and separation.
I hope this helps you with your research. For more details, you can refer to the sources I mentioned by their numerical references.
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