Notes

<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/2.1" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/2.1 http://www.xrdml.com/XRDMeasurement/2.1/XRDMeasurement.xsd" status="Completed">
<comment>
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=8/25/2016 12:17:20 PM</entry>
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
<entry>Diffractometer system=EMPYREAN</entry>
<entry>Measurement program=C:PANalyticalData CollectorProgramsspinnerSi-spinner-standaardmeting.xrdmp, Identifier={...}</entry>
<entry>Batch program=C:PANalyticalData CollectorProgramsspinnerbatch-7samples.xrdmp, Identifier={...}</entry>
</comment>
<sample type="To be analyzed">
<id>2020-0684</id>
<name>20-152 sample 1: ....</name>
<preparedBy></preparedBy>
</sample>
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
<comment>
<entry>Spinner - beam knife</entry>
<entry>PHD Lower Level = 3.81 (keV), PHD Upper Level = 9.70 (keV)</entry>
</comment>
<usedWavelength intended="K-Alpha 1">
<kAlpha1 unit="Angstrom">1.7890100</kAlpha1>
<kAlpha2 unit="Angstrom">1.7929000</kAlpha2>
<kBeta unit="Angstrom">1.6208300</kBeta>
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
</usedWavelength>
<incidentBeamPath>
<radius unit="mm">240.00</radius>
<xRayTube id="1010055" name="Empyrean Co LFF HR (9430 033 7613x) DK423981">
<tension unit="kV">40.0</tension>
<current unit="mA">45.0</current>
<anodeMaterial>Co</anodeMaterial>
<focus type="Line">
<length unit="mm">12.0</length>
<width unit="mm">0.4</width>
<takeOffAngle unit="deg">7.8</takeOffAngle>
</focus>
</xRayTube>
<xRayMirror id="27020010" name="Bragg-Brentano HD Co" hybrid="false">
<crystal type="Graded" shape="Flat">BB/HD</crystal>
<acceptanceAngle unit="deg">1.339</acceptanceAngle>
<length unit="mm">55.3</length>
</xRayMirror>
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
<opening unit="rad">0.0400</opening>
</sollerSlit>
<mask id="22030010" name="Fixed mask 20 mm">
<distanceToSample unit="mm">171.20</distanceToSample>
<width unit="mm">20.00</width>
</mask>
<antiScatterSlit id="22010002" name="Fixed slit 2°" xsi:type="fixedAntiScatterSlitType">
<height unit="mm">3.03</height>
</antiScatterSlit>
<divergenceSlit id="22010004" name="Fixed slit 1/2°" xsi:type="fixedDivergenceSlitType">
<distanceToSample unit="mm">179.50</distanceToSample>
<height unit="mm">0.76</height>
</divergenceSlit>
</incidentBeamPath>
<beamKnife id="29030011" name="Beam knife for linear detectors"/>
<sampleMovement xsi:type="spinningSampleMovementType">
<spinnerRevolutionTime unit="seconds">1.0</spinnerRevolutionTime>
</sampleMovement>
<sampleOffset>
<position axis="2Theta" unit="deg">0.0000</position>
<position axis="Omega" unit="deg">0.0000</position>
</sampleOffset>
<diffractedBeamPath>
<radius unit="mm">240.00</radius>
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="fixedAntiScatterSlitType">
<angle unit="deg">1</angle>
</antiScatterSlit>
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
<opening unit="rad">0.0400</opening>
</sollerSlit>
<detector id="7010020" name="PIXcel3D-Medipix3 1x1 detector" xsi:type="areaDetectorType">
<phd unit="%">
<lowerLevel>27.5</lowerLevel>
<upperLevel>70.0</upperLevel>
</phd>
<mode>Scanning</mode>
<activeChannelsEquatorial>255</activeChannelsEquatorial>
<activeChannelsAxial>255</activeChannelsAxial>
<pitchEquatorial unit="mm">0.05500</pitchEquatorial>
<pitchAxial unit="mm">0.05500</pitchAxial>
<readOutPeriod unit="seconds">0.195</readOutPeriod>
</detector>
</diffractedBeamPath>
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
<header>
<startTimeStamp>2020-06-04T18:32:55+02:00</startTimeStamp>
<endTimeStamp>2020-06-04T19:02:33+02:00</endTimeStamp>
<author>
<name>XRD2</name>
</author>
<source>
<applicationSoftware version="6.1">Data Collector</applicationSoftware>
<instrumentControlSoftware version="8.1 20181218">EMPYREAN</instrumentControlSoftware>
<instrumentID>0000000011184151</instrumentID>
</source>
</header>
<dataPoints>
<positions axis="2Theta" unit="deg">
<startPosition>5.01156514</startPosition>
<endPosition>119.99345054</endPosition>
</positions>
<positions axis="Omega" unit="deg">
<startPosition>2.50578257</startPosition>
<endPosition>59.99672527</endPosition>
</positions>
<positions axis="Phi" unit="deg">
<commonPosition>20.9</commonPosition>
</positions>
<commonCountingTime unit="seconds">48.195</commonCountingTime>

</dataPoints>
</scan>
</xrdMeasurement>
</xrdMeasurements>